Title
Creep strength of nickel oxide/zirconia composites under different environmental atmospheres
Date Issued
04 October 2012
Access level
metadata only access
Resource Type
conference paper
Author(s)
Jiménez-Melendo M.
Universidad de Sevilla
Abstract
NiO/8YSZ (8 mol% Y 2O 3-stabilized cubic ZrO 2) and NiO/3YTZP (3 mol% Y 2O 3-stabilized tetragonal ZrO 2) composites with different NiO contents have been fabricated by a conventional route of mechanical mixing of NiO and zirconia powders and sintering at 1500 °C for 10 h in air. The resulting microstructures have been characterized by electron microscopy. The composites show a duplex microstructure formed by equiaxed grains of NiO and ZrO 2, without any intermediate phase. Compressive mechanical tests at constant strain rate were carried out at temperatures between 1150 and 1350 °C under different environments: air, inert (Ar) and reducing (5% H 2/95% Ar) atmospheres. The overall creep behavior of the composites is essentially controlled by the zirconia matrix, due to the softness of the NiO phase in the experimental conditions used in this study. The creep strength is not affected by oxygen partial pressure. However, a large decrease in creep resistance under reducing conditions was observed in samples submitted to in situ redox cycling. © 2012 Elsevier B.V.
Start page
471
End page
475
Volume
225
Language
English
OCDE Knowledge area
Física de la materia condensada
Scopus EID
2-s2.0-84867577951
Source
Solid State Ionics
ISSN of the container
01672738
Sources of information: Directorio de Producción Científica Scopus