Title
Influence of pH on crystal phase formation in BaTiO3 nanoparticles during their peroxide synthesis
Date Issued
01 January 2022
Access level
metadata only access
Resource Type
journal article
Author(s)
Emelianov N.A.
Budaev A.V.
Azahuanche F.R.P.
Lopez J.A.R.
Publisher(s)
Taylor and Francis Ltd.
Abstract
Influence of pH of the medium on the crystal phases formation in BaTiO3 nanoparticles during their peroxide synthesis has been investigated. Nanoparticles in the ferroelectric tetragonal phase are formed at pH 9 when annealed at temperatures above 900 °C. Decreasing pH value to 8 leads to formation of nanoparticles in paraelectric cubic phase, while increasing the annealing temperature to 1100 °C does not lead to formation of other crystalline phases. Increasing pH value to 10 results in the formation of Ba2TiO4 and BaTi4O9 in addition to BaTiO3.
Start page
206
End page
212
Volume
590
Issue
1
Language
English
OCDE Knowledge area
Nano-procesos Nano-materiales
Scopus EID
2-s2.0-85132996602
Source
Ferroelectrics
ISSN of the container
00150193
Sponsor(s)
This work was supported by the grant from the President of the Russian Federation for state support of young Russian scientists–candidates of science (MK-3916.2021.1.2). The authors are grateful to Prof. L. N. Korotkov (Voronezh State Technical University) for a fruitful discussion of this research.
Sources of information: Directorio de Producción Científica Scopus