Title
Detection of nutshells in cumin powder using NIR hyperspectral imaging and chemometrics tools
Date Issued
01 May 2022
Access level
metadata only access
Resource Type
journal article
Author(s)
Publisher(s)
Academic Press Inc.
Abstract
Cumin is a valuable spice for medical and food applications. Nevertheless, reports of the presence of undeclared adulterants in cumin require the development of analytical methods for its authentication. The goal of this study was to develop a new analytical method based on NIR-HSI (900–1710 nm) and chemometrics to detect low-cost adulterants peanut shell, pecan shell and walnut shell in cumin. PCA was applied to investigate the spectral features of pure samples and mixtures. Soft Independent Modelling Class Analogy (SIMCA) was applied to classify pure cumin and adulterated samples, achieving an accuracy of 95 % for test samples. Partial Least Square Regression (PLSR) model based on selected variables using iPLS or GA showed a similar (for walnut shell) or better (peanut and pecan shell) performance than PLSR models based on a full wavelength with detection limits above 1% and RPD (Residual Prediction Deviation) values higher than 5, indicating excellent predictive ability. Chemical maps allow visualization of shell concentration and distribution in cumin samples. This work demonstrated the potential of NIR-HSI and chemometrics to detect and quantify nutshells in cumin powder.
Volume
108
Language
English
OCDE Knowledge area
Electroquímica
Alimentos y bebidas
Subjects
Scopus EID
2-s2.0-85123259470
Source
Journal of Food Composition and Analysis
ISSN of the container
08891575
Sources of information:
Directorio de Producción Científica
Scopus