Title
Quantitative three-dimensional fractography in sapphire fibers
Date Issued
01 January 2007
Access level
metadata only access
Resource Type
conference paper
Author(s)
University of Seville
Abstract
The usual methods of choice for fractographic analysis are regular light microscopy, often with interference contrast, and scanning electron microscopy (SEM). However, several other microscopic techniques are also useful. One such technique is confocal microscopy (LSCM); capable of height discrimination, of wide-area imaging and ideally suited to quantitative analysis, LSCM has an excellent synergy with SEM. In this paper, LSCM will be used to study the fracture surface of single-crystal sapphire fibers under subcritical crack growth (SCG). When SCG is present, several distinct zones may be identified in the fracture surface: the subcritical zone, the mirror zone, and the branching zone. In the branching zone, the fracture follows a restricted set of "easy" crystalline planes on its propagation, resembling a mountain range where the possible orientations of the slopes are restricted. These fibers have already been studied with SEM, but the shortcomings of the electron microscope restrict the possible studies. In addition to reflection-mode observation, a simple experimental method which allows for fluorescent-mode usage at virtually no economic cost will be introduced. 3D models of the distinct zones of the fracture surface will be built and quantitatively analyzed with profiles and histograms. As compared with SEM, the unique information obtained includes perspective views of the fracture surface, clear SCG-mirror boundary contrast, overall surface orientation statistics, height profiles and easy mirror-zone-limit determination, all with a technique which is fast, non-destructive and which requires almost no sample preparation.
Start page
67
End page
77
Volume
199
Language
English
OCDE Knowledge area
Física de la materia condensada
Ingeniería de materiales
Scopus EID
2-s2.0-57649238363
Source
Ceramic Transactions
Resource of which it is part
Ceramic Transactions
ISSN of the container
10421122
ISBN of the container
978-047009737-3
Conference
Ceramic Transactions
Sponsor(s)
I acknowledge the generous support of The European Research Council (ERC-2013-CoG, 617970, CARP) during the research for this article (2014\u20132018). The European Union\u2019s Horizon 2020 research and innovation program under the Marie Sk\u0142odowska-Curie Global Fellowship (Grant Agreement No. 101031711) provided funding while I was writing this article. A previous iteration titled \u201CImages on the Move: Migrant Saints \u2018Beyond\u2019 the Mexico-US Border\u201D won the JB Donne Essay Prize on the Anthropology of Art in 2019. I am very thankful to the Royal Anthropological Institute for this award and providing this oppor-tunity to explore the ideas appearing in this piece. My most heartfelt gratitude goes to Manuela, Ana Hern\u00E1ndez, and the members of the art collective The Tlacolulokos, Dar\u00EDo Canul and Cosijoesa Cernas, for graciously and generously sharing their stories and photos with me. Muchas gracias a todos ustedes. Different versions of this article have also greatly benefited from the invaluable insights provided by colleagues among which Charles Stewart, Kristin Norget, Peter Wogan, Tarek Elhaik, Michael Herzfeld, Dav\u00EDd Carrasco, and Eleana Yalouri. I am very grateful for their feedback. I am also obliged Chihab El Khachab for his invitation to present an unpolished version of this paper at Oxford University, as well as for the enthusiastic and enlightening conversations that ensued, especially with Clare Harris, Dolorez Martinez, and David Zeitlyn. Many thanks are also due to the AQ editor, Roy Richard Grinker, and the anonymous reviewers of Anthropological Quarterly for their invaluable comments, and to Alexander Hall for his meticulous editing of an earlier iteration of this article. Finally, I extend my gratitude to the talented Jeff McLane for sharing his stunning photographs of the Tlacolulokos\u2019 art and their exhibition, \u201CVisualizing Language: Oaxaca in L.A.\u201D at the Los Angeles Public Library.
during the research for this article (2014\u20132018). The European Union\u00BBs /orizon 2020 research and innovation program under the Marie Sk\u00E9odowska-Curie Global Fellowship (Grant Agreement No. 101031711) provided funding while I was writing this article. A previous iteration titled \u201CImages on the Move: Migrant Saints \u00BABeyond\u00BB the Mexico-US Border\u201D won the JB Donne Essay Prize on the Anthropology of Art in 2019. I am very thankful to the Royal Anthropological Institute for this award and providing this oppor-tunity to explore the ideas appearing in this piece. My most heartfelt gratitude goes to Manuela, Ana /ernmndez, and the members of the art collective The Tlacolulokos, Darxo Canul and Cosijoesa Cernas, for graciously and generously sharing their stories and photos with me. Muchas gracias a todos ustedes.
Sources of information:
Directorio de Producción Científica
Scopus