Title
Microstructure and Tensile Properties of Fine-Grained Bulk Copper Fabricated by Thermomechanical Consolidation of Copper Nanopowder/Micron-Sized Powder Blend
Date Issued
01 January 2022
Access level
open access
Resource Type
journal article
Author(s)
Bhatta G.
De Los Santos Valladares L.
Moreno N.O.
Barnes C.H.W.
Chen W.
Zhang D.
Publisher(s)
Universidade Federal de Sao Carlos
Abstract
Samples of fine structured Cu were fabricated by spark plasma sintering (SPS) of compacts of Cu nanopowder/micron-sized powder blend with a ratio of 3:7 by weight, and one of the SPSed samples was further processed by hot extrusion. The microstructures of the as-SPSed and the as-extruded samples and the tensile properties and fracture behavior of the as-extruded sample were studied. It was found that the microstructures of the samples consist of a concoction of ultrafine and coarse grains with high dislocation densities ( ~ 1015 m-2) as a result of microstructural evolution during material processing. Some nanograins were oxidized to form Cu2O particles residing around the coarse grains. Extrusion of the SPSed sample increases its microhardness from 70 HV to 90 HV. The electrical conductivity of the as-extruded sample reaches 87% international annealed copper standard (IACS), and its tensile properties are 200 MPa for yield strength, 218 MPa for ultimate tensile strength and 9% for elongation to fracture. The tensile test specimens from the as-extruded sample exhibit nearly ideal plastic deformation and undergo ductile fracture, suggesting that the fine-grained copper is a highly desirable material for high strength electrical conductors.
Volume
25
Language
English
OCDE Knowledge area
Física de la materia condensada Nano-materiales
Scopus EID
2-s2.0-85122884137
Source
Materials Research
ISSN of the container
15161439
Sponsor(s)
G. Bhatta and D. Zhang thank the financial support from China Scholarship Council (CSC) (grant nos. 2017GXZ026346) and the "Xing Liao Talent Plan" of Liaoning Province, China (Project No. XLYC1802080) to the work in China. The work in Peru has been supported by the Incorporación de Investigadores Program from the CONCYTEC - FONDECYT - UNMSM (Contract No. 12-2019 - FONDECYT - BM - INC. INV.).
Sources of information: Directorio de Producción Científica Scopus