Title
Fabrication and creep properties of eutectic-composition Al<inf>2</inf>O<inf>3</inf>/YAG/YSZ sintered composites
Date Issued
01 December 2021
Access level
metadata only access
Resource Type
journal article
Author(s)
Publisher(s)
Elsevier Ltd
Abstract
Three-phase alumina/YAG/yttria-stabilized cubic zirconia (YSZ) composites were fabricated by a solid-state reaction route starting from commercial powders of Al2O3, Y2O3 and monoclinic ZrO2. The final phases Al2O3, YAG and YSZ were obtained after calcination of the powder mixtures at 1400 °C. Dense bulk composites were obtained after sintering, with a homogeneous microstructure of fine and equiaxed grains with sizes of 1 μm. Compressive mechanical tests were performed at 1300–1450 °C in air at constant load and at constant initial strain rate. A brittle-to-ductile transition was found with increasing temperature. Grain boundary sliding is the main deformation mechanism in the ductile regime, characterized by a stress exponent of 2 and by the absence of dislocation activity and changes in grain morphology. Alumina seems to be the rate-controlling phase owing to the improvement in creep resistance by the presence of yttrium and zirconium of the other two phases.
Start page
7752
End page
7761
Volume
41
Issue
15
Language
English
OCDE Knowledge area
Física de la materia condensada
Cerámica
Subjects
Scopus EID
2-s2.0-85111979529
Source
Journal of the European Ceramic Society
ISSN of the container
09552219
Sponsor(s)
This work was supported by the Project no. MAT2009-13979-C03-01, Ministerio de Ciencia e Innovación, Spain .
Sources of information:
Directorio de Producción Científica
Scopus